Silver ion chromatography using solid-phase extraction columns packed with a bonded-sulfonic acid phase.

نویسنده

  • W W Christie
چکیده

Commercial solid-phase extraction columns packed with a stationary phase with bonded benzenesulfonic acid groups are readily converted to the silver ion form and can then be used for silver ion chromatography of lipids. To illustrate the utility of such procedures, methyl ester derivatives of fatty acids with zero to six double bonds were separated from each other by a simple stepwise elution scheme. -Christie, W. W. Silver ion chromatography using solid-phase extraction columns packed with a bonded-sulfonic acid phase.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Solid-Phase Extraction Columns for Lipid Analysis

Solid-phase extraction methods are being used for increasing numbers of applications in lipid analysis, but especially as a rapid means of isolating particular components for further analysis. Many different types of packing material are available enabling most different modes of chromatography to be used, including adsorption, reversed-phase, silver-ion and ion-exchange. However, there are occ...

متن کامل

Multiresidue determination of organophosphorus pesticides in corn oil using solid-phase extraction with lanthanum silicate sorbent and gas chromatography

Phosalone, malathion and diazinon were analyzed in corn oil using solid phase extraction (SPE)with lanthanum silicate as a new solid sorbent followed by gas chromatography with nitrogenphosphorus detection (GC-NPD). The efficiency of different eluents (methanol, dichloromethane,ethyl acetate, dichloromethane — ethyl acetate (1:1) and ethyl acetate — methanol (1:1)) werecompared for elution of o...

متن کامل

Microsequence analysis: I. Peptide isolation using high-performance liquid chromatography.

Peptide mixtures, arising from such diverse sources as tissue extracts, urine or proteolysis, are usually fractionated and characterized by a combination of ion-exchange chromatography, gel-exclusion chromatography and/or electrophoresis. Appropriate combinations of these methods will normally yield a homogeneous product, but their costs, detection limits, analyses times and yields vary. The re...

متن کامل

A Nano-Composite Based on Fe3O4@Styrene-Maleic Anhydride Copolymer as a Magnetic Sorbent for Preconcentration of Silver(I) Ion

A magnetic nano-composite based on modified styren-maleic anhydride copolymer and Fe3O4 nano-particles was introduced as a new sorbent for solid-phase extraction and preconcentration of trace levels of silver ion from aqueous solutions. The size and morphology of the nano-sorbent were characterized via X-ray diffraction analysis, scanning electron microscopy and Fourier transform infrared spect...

متن کامل

Preconcentration and Determination of Mefenamic Acid in Pharmaceutical and Biological Fluid Samples by Polymer-grafted Silica Gel Solid-phase Extraction Following High Performance Liquid Chromatography

Abstract Mefenamic acid is a nonsteroidal anti-inflammatory drug (NSAID) that has analgesic,anti-infammatory and antipyretic actions. It is used to relieve mild to moderate pains. Solid-phase extraction of mefenamic acid by a polymer grafted to silica gel is reported . Poly allyl glycidyl ether/iminodiacetic acid-co-N, N-dimethylacrylamide was synthesized and grafted to silica gel and was used ...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:
  • Journal of lipid research

دوره 30 9  شماره 

صفحات  -

تاریخ انتشار 1989